(S)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine

Base Information

Chemical Name:(S)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine
CAS No.:129757-63-7
Molecular Formula:C₂₀H₂₃N₃O₅
Molecular Weight:385.42
Hs Code.:

Synonyms:(S)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine

Suppliers and Price of (S)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine

Chemical Property:

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Technology Process of (S)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine

There total 6 articles about (S)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 663600-32-6
1-phenethyl-pentylamine

: 99-33-2
3,5-dinitrobenoyl chloride

: 129757-59-1
(R)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine

: 129757-63-7
(S)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; optical yield given as %ee;
DOI:10.1002/adsc.200800017

Reference yield:

: 129757-50-2
N-((S)-2,2-Dimethyl-1-phenethyl-propyl)-N-[(S)-2-(2-methoxy-ethoxymethyl)-pyrrolidin-1-yl]-acetamide

: 129757-63-7
(S)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / lithium, NH₃ (liquid) / tetrahydrofuran / 1 h / -33 °C

With ammonia; lithium; In tetrahydrofuran;
DOI:10.1021/jo00312a034

Reference yield:

: 127221-99-2
(2S,3''R)-1-[N-(1-butyl-3-phenylpropyl)-N-methoxycarbonylamino]-2-(2-methoxy ethoxymethyl)pyrrolidine

: 129757-63-7
(S)-N-(3,5-dinitrobenzoyl)-α-butylbenzenepropanamine

Guidance literature:: Multi-step reaction with 2 steps

1: lithium, NH₃ (liquid) / tetrahydrofuran / 1 h / -33 °C

2: 1) iodotrimethylsilane 2) Et₃N / 1a) CH₃CN, RT, 1 h, 1b) MeOH, 20 min, 2) CH₂CL₂, RT

With trimethylsilyl iodide; ammonia; lithium; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00312a034