the dicamphorsulfonate of (1S,2S,4S,5S)-2,5-diphenylcyclohexane-1,4-diol

Base Information

Chemical Name:the dicamphorsulfonate of (1S,2S,4S,5S)-2,5-diphenylcyclohexane-1,4-diol
CAS No.:112070-18-5
Molecular Formula:C₃₈H₄₈O₈S₂
Molecular Weight:696.926
Hs Code.:

Synonyms:the dicamphorsulfonate of (1S,2S,4S,5S)-2,5-diphenylcyclohexane-1,4-diol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of the dicamphorsulfonate of (1S,2S,4S,5S)-2,5-diphenylcyclohexane-1,4-diol

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Technology Process of the dicamphorsulfonate of (1S,2S,4S,5S)-2,5-diphenylcyclohexane-1,4-diol

There total 4 articles about the dicamphorsulfonate of (1S,2S,4S,5S)-2,5-diphenylcyclohexane-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 21286-54-4
(+)-(1S)-Campher-10-sulfonsaeure-chlorid

: (1R,2S,4R,5S)-2,5-Diphenyl-cyclohexane-1,4-diol

: 112070-18-5
the dicamphorsulfonate of (1S,2S,4S,5S)-2,5-diphenylcyclohexane-1,4-diol

Guidance literature:: With pyridine; at 0 ℃; for 2h;
DOI:10.1021/ja00260a037

Reference yield:

: 23402-69-9
lithium diphenylcuprate

: 112070-18-5
the dicamphorsulfonate of (1S,2S,4S,5S)-2,5-diphenylcyclohexane-1,4-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / diethyl ether; various solvent(s) / 12 h / -45 deg C up to RT

2: 99 percent / pyridine / 2 h / 0 °C

With pyridine; In diethyl ether;
DOI:10.1021/ja00260a037

Reference yield:

: trans-2-phenyl-4-cyclohexenol

: 112070-18-5
the dicamphorsulfonate of (1S,2S,4S,5S)-2,5-diphenylcyclohexane-1,4-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / (CH₃)3COOH, Mo(CO)6 / toluene / 2.5 h / 60 °C

2: 73 percent / diethyl ether; various solvent(s) / 12 h / -45 deg C up to RT

3: 99 percent / pyridine / 2 h / 0 °C

With pyridine; tert.-butylhydroperoxide; hexacarbonyl molybdenum; In diethyl ether; toluene;
DOI:10.1021/ja00260a037