1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N³-benzyluracil

Base Information

Chemical Name:1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N³-benzyluracil
CAS No.:161824-87-9
Molecular Formula:C₂₃H₂₄N₂O₆
Molecular Weight:424.453
Hs Code.:

1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N<sup>3</sup>-benzyluracil

Synonyms:1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N³-benzyluracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N³-benzyluracil

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Technology Process of 1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N³-benzyluracil

There total 6 articles about 1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N³-benzyluracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3,5'-dibenzyl-2',3'-O–isopropylidene uridine

: 161824-87-9
1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N³-benzyluracil

Guidance literature:: With trifluoroacetic acid; In dichloromethane; water; at 20 ℃; for 4h;
DOI:10.3390/molecules25235513

Reference yield: 85.0%

: 161824-84-6
1-(2'-O,3'-O-Cyclopentyl-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N³-benzyluracil

: 161824-87-9
1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N³-benzyluracil

Guidance literature:: With trifluoroacetic acid; at 0 ℃; for 0.333333h;
DOI:10.1021/jo00103a017

Reference yield:

: 58-96-8
uridine

: 161824-87-9
1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N³-benzyluracil

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 0.42 h / 90 °C

2: 93 percent / NaH / 1,2-dimethoxy-ethane / 1.) r.t., 2.) 90 deg C, 10 h

3: 85 percent / 30percent aq. TFA / 0.33 h / 0 °C

With sodium hydride; toluene-4-sulfonic acid; trifluoroacetic acid; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00103a017