1-O-benzoyl-2-O-acetyllycorine

Base Information

• Chemical Name: 1-O-benzoyl-2-O-acetyllycorine
• CAS No.: 1248343-27-2
• Molecular Formula: C₂₅H₂₃NO₆
• Molecular Weight: 433.461
• Mol file: 1248343-27-2.mol

Synonyms:1-O-benzoyl-2-O-acetyllycorine

Chemical Property of 1-O-benzoyl-2-O-acetyllycorine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-O-benzoyl-2-O-acetyllycorine

There total 1 articles about 1-O-benzoyl-2-O-acetyllycorine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(1S,2S,3a(1)S,12bS)-2-hydroxy-2,3a(1),4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1-yl benzoate (1248343-26-1) + acetic anhydride (108-24-7) → 1-O-benzoyl-2-O-acetyllycorine (1248343-27-2)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1016/j.bmcl.2010.06.130

upstream raw materials:

(1S,2S,3a⁽¹⁾S,12bS)-2-hydroxy-2,3a⁽¹⁾,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1-yl benzoate

acetic anhydride