Cyclopropanecarboxamide, 1-(acetyloxy)-2-methyl-, cis- (9CI)

Base Information

Chemical Name:Cyclopropanecarboxamide, 1-(acetyloxy)-2-methyl-, cis- (9CI)
CAS No.:123032-99-5
Molecular Formula:C₇H₁₁NO₃
Molecular Weight:157.169
Hs Code.:
Mol file:123032-99-5.mol

Synonyms:Cyclopropanecarboxamide, 1-(acetyloxy)-2-methyl-, cis- (9CI)

Suppliers and Price of Cyclopropanecarboxamide, 1-(acetyloxy)-2-methyl-, cis- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Cyclopropanecarboxamide, 1-(acetyloxy)-2-methyl-, cis- (9CI)

Chemical Property:

PSA：69.39000
LogP:0.51370

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclopropanecarboxamide, 1-(acetyloxy)-2-methyl-, cis- (9CI)

There total 3 articles about Cyclopropanecarboxamide, 1-(acetyloxy)-2-methyl-, cis- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (1S,2R)-1-chlorocarbonyl-2-methyl-cyclopropyl ester

: 123032-99-5
Acetic acid (1S,2R)-1-carbamoyl-2-methyl-cyclopropyl ester

Guidance literature:: With ammonia; In 1,4-dioxane; for 1h; Yield given; Ambient temperature;
DOI:10.1055/s-1989-27220

Reference yield:

: 123032-92-8
(1S,2R)-1-Acetoxy-2-methyl-cyclopropanecarboxylic acid

: 123032-99-5
Acetic acid (1S,2R)-1-carbamoyl-2-methyl-cyclopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, DMF / 2 h / 50 °C

2: NH₃ / dioxane / 1 h / Ambient temperature

With thionyl chloride; ammonia; N,N-dimethyl-formamide; In 1,4-dioxane;
DOI:10.1055/s-1989-27220

Reference yield:

: 39590-72-2,59322-54-2,112835-85-5,112835-87-7,118865-70-6
(1S,2R)-1-Hydroxy-2-methyl-cyclopropanecarboxylic acid

: 123032-99-5
Acetic acid (1S,2R)-1-carbamoyl-2-methyl-cyclopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / 1 h / Heating

2: SOCl₂, DMF / 2 h / 50 °C

3: NH₃ / dioxane / 1 h / Ambient temperature

With thionyl chloride; ammonia; N,N-dimethyl-formamide; In 1,4-dioxane;
DOI:10.1055/s-1989-27220