N-tert-butyl-2-(3-amino-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-⁽¹⁾benzazepin-1-yl)-ethanoic acid amide

Base Information

• Chemical Name: N-tert-butyl-2-(3-amino-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-⁽¹⁾benzazepin-1-yl)-ethanoic acid amide
• CAS No.: 152607-18-6
• Molecular Formula: C₂₂H₂₇N₃O₂
• Molecular Weight: 365.475

Synonyms:N-tert-butyl-2-(3-amino-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-⁽¹⁾benzazepin-1-yl)-ethanoic acid amide

Chemical Property of N-tert-butyl-2-(3-amino-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-⁽¹⁾benzazepin-1-yl)-ethanoic acid amide

Chemical Property:

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Technology Process of N-tert-butyl-2-(3-amino-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-⁽¹⁾benzazepin-1-yl)-ethanoic acid amide

There total 1 articles about N-tert-butyl-2-(3-amino-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-⁽¹⁾benzazepin-1-yl)-ethanoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tert-butyl-2-[3-azido-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-(1)benzazepin-1-yl] ethanoic acid amide (152607-17-5) → N-tert-butyl-2-(3-amino-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-(1)benzazepin-1-yl)-ethanoic acid amide (152607-18-6)

Guidance literature:

With H₂; palladium-carbon; In methanol;

Reference yield:

N-tert-butyl-2-(3-amino-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-(1)benzazepin-1-yl)-ethanoic acid amide (152607-18-6) + 3-tolyl isocyanate (621-29-4) → N-tert-butyl-2-[3-(3-(3-tolyl)ureido)-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-(1)benzazepin-1-yl] ethanoic acid amide (152607-14-2)

Guidance literature:

With N₂; In dichloromethane;

upstream raw materials:

N-tert-butyl-2-[3-azido-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-⁽¹⁾benzazepin-1-yl] ethanoic acid amide

Downstream raw materials:

N-tert-butyl-2-[3-(3-(3-tolyl)ureido)-2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-⁽¹⁾benzazepin-1-yl] ethanoic acid amide

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