Formic acid 1-[6-(2,4-dichloro-phenyl)-pyridazin-3-yl]-piperidin-4-yl ester

Base Information

Chemical Name:Formic acid 1-[6-(2,4-dichloro-phenyl)-pyridazin-3-yl]-piperidin-4-yl ester
CAS No.:99708-35-7
Molecular Formula:C₁₆H₁₅Cl₂N₃O₂
Molecular Weight:352.22
Hs Code.:

Synonyms:Formic acid 1-[6-(2,4-dichloro-phenyl)-pyridazin-3-yl]-piperidin-4-yl ester

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Chemical Property of Formic acid 1-[6-(2,4-dichloro-phenyl)-pyridazin-3-yl]-piperidin-4-yl ester

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Technology Process of Formic acid 1-[6-(2,4-dichloro-phenyl)-pyridazin-3-yl]-piperidin-4-yl ester

There total 4 articles about Formic acid 1-[6-(2,4-dichloro-phenyl)-pyridazin-3-yl]-piperidin-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2565-30-2
formyl chloride

: 93181-85-2
1 [6 (2,4 dichlorophenyl) 3 pyridazinyl] 4 piperidinol

: 99708-35-7
Formic acid 1-[6-(2,4-dichloro-phenyl)-pyridazin-3-yl]-piperidin-4-yl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; for 18h; Heating;
DOI:10.1021/jm00153a011

Reference yield:

: 5382-16-1
4-HYDROXYPIPERIDINE

: 99708-35-7
Formic acid 1-[6-(2,4-dichloro-phenyl)-pyridazin-3-yl]-piperidin-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / butan-1-ol / 3 h / Heating

2: 60 percent / Et₃N / tetrahydrofuran / 18 h / Heating

With triethylamine; In tetrahydrofuran; butan-1-ol;
DOI:10.1021/jm00153a011

Reference yield:

: 93181-86-3
3-chloro-6-(2,4-dichlorophenyl)pyridazine

: 99708-35-7
Formic acid 1-[6-(2,4-dichloro-phenyl)-pyridazin-3-yl]-piperidin-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / butan-1-ol / 3 h / Heating

2: 60 percent / Et₃N / tetrahydrofuran / 18 h / Heating

With triethylamine; In tetrahydrofuran; butan-1-ol;
DOI:10.1021/jm00153a011