(Z)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol

Base Information

Chemical Name:(Z)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol
CAS No.:76042-69-8
Molecular Formula:C₁₉H₃₄O₂
Molecular Weight:294.478
Hs Code.:

Synonyms:(Z)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol

Suppliers and Price of (Z)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol

There total 11 articles about (Z)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76042-84-7
2-(6-Butyl-7-oxa-bicyclo[4.1.0]hept-1-yl)-1-pentyl-cyclobutanol

: 76042-69-8
(Z)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol

: 76042-70-1
(E)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol

Guidance literature:: With magnesium methanolate; In methanol; at 2 ℃; for 72h; Yield given. Yields of byproduct given;
DOI:10.1021/ja00547a015

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 76042-69-8
(Z)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol

Guidance literature:: Multi-step reaction with 7 steps

1: 86 percent / lithium diisopropylamide / tetrahydrofuran / -78 °C

2: 1.) phosphorus oxychloride, HMPA, 2.) pyridine / 1.) room temperature -> 50 deg C, 2.) 50 deg C -> 100 deg C

3: 66 percent / diethyl ether / Ambient temperature

4: 48 percent / 48percent fluoboric acid / diethyl ether

5: 79 percent / diethyl ether / 3 h / -78 deg C -> room temperature

6: MCPBA, 0.5 M sodium bicarbonate / CH₂Cl₂ / 5 h / 0 °C

7: magnesium methoxide / methanol / 72 h / 2 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrafluoroboric acid; sodium hydrogencarbonate; magnesium methanolate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; trichlorophosphate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1021/ja00547a015

Reference yield:

: 76042-34-7
2-(2-n-butylcyclohexen-1-yl)cyclobutanone

: 76042-69-8
(Z)-2-(4-oxo-n-nonylidene)-1-n-butylcyclohexanol

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / diethyl ether / 3 h / -78 deg C -> room temperature

2: MCPBA, 0.5 M sodium bicarbonate / CH₂Cl₂ / 5 h / 0 °C

3: magnesium methoxide / methanol / 72 h / 2 °C

With sodium hydrogencarbonate; magnesium methanolate; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/ja00547a015