2,3,5,6-tetrahydro-4-hydroxyimino-3,5-dioxo-2-phenethyl-1,2,6-thiadiazine 1,1-dioxide, sodium salt monohydrate

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Chemical Name:2,3,5,6-tetrahydro-4-hydroxyimino-3,5-dioxo-2-phenethyl-1,2,6-thiadiazine 1,1-dioxide, sodium salt monohydrate
CAS No.:106350-07-6
Molecular Formula:C₁₁H₁₀N₃O₅S*Na
Molecular Weight:319.273
Hs Code.:

Synonyms:2,3,5,6-tetrahydro-4-hydroxyimino-3,5-dioxo-2-phenethyl-1,2,6-thiadiazine 1,1-dioxide, sodium salt monohydrate

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Chemical Property of 2,3,5,6-tetrahydro-4-hydroxyimino-3,5-dioxo-2-phenethyl-1,2,6-thiadiazine 1,1-dioxide, sodium salt monohydrate

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Technology Process of 2,3,5,6-tetrahydro-4-hydroxyimino-3,5-dioxo-2-phenethyl-1,2,6-thiadiazine 1,1-dioxide, sodium salt monohydrate

There total 2 articles about 2,3,5,6-tetrahydro-4-hydroxyimino-3,5-dioxo-2-phenethyl-1,2,6-thiadiazine 1,1-dioxide, sodium salt monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 106350-03-2
2,3,5,6-tetrahydro-3,5-dioxo-2-phenethyl-1,2,6-thiadiazine 1,1-dioxide

: 106350-07-6
2,3,5,6-tetrahydro-4-hydroxyimino-3,5-dioxo-2-phenethyl-1,2,6-thiadiazine 1,1-dioxide, sodium salt monohydrate

Guidance literature:: With acetic acid; sodium nitrite; In 1,4-dioxane; water; 1) 1 h, 0 deg C, 2) RT;

Reference yield:

: 710-15-6
N-Phenethylsulfamide

: 106350-07-6
2,3,5,6-tetrahydro-4-hydroxyimino-3,5-dioxo-2-phenethyl-1,2,6-thiadiazine 1,1-dioxide, sodium salt monohydrate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / toluene

2: 78 percent / acetic acid, sodium nitrite / dioxane; H₂O / 1) 1 h, 0 deg C, 2) RT

With acetic acid; sodium nitrite; In 1,4-dioxane; water; toluene;