2-(2-aminophenyl)-5-ethylfuran

Base Information

Chemical Name:2-(2-aminophenyl)-5-ethylfuran
CAS No.:1045704-66-2
Molecular Formula:C₁₂H₁₃NO
Molecular Weight:187.241
Hs Code.:

Synonyms:2-(2-aminophenyl)-5-ethylfuran

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Chemical Property of 2-(2-aminophenyl)-5-ethylfuran

Chemical Property:

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Technology Process of 2-(2-aminophenyl)-5-ethylfuran

There total 4 articles about 2-(2-aminophenyl)-5-ethylfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1045704-62-8
2-acetyl-5-(2-nitrophenyl)-furan

: 1045704-66-2
2-(2-aminophenyl)-5-ethylfuran

Guidance literature:: With water; nickel; hydrazine; In ethanol; Reflux;
DOI:10.1055/s-2008-1072720

Reference yield:

: 56656-34-9
1-(5-(2-nitrophenyl)furan-2-yl)ethanone

: 1045704-66-2
2-(2-aminophenyl)-5-ethylfuran

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃; NaBH₄ / tetrahydrofuran / Heating

2: hydrazin hydrate / Raney nickel / ethanol / Heating

With sodium tetrahydroborate; aluminium trichloride; hydrazine hydrate; nickel; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tetlet.2006.04.080

Reference yield:

: 1192-62-7,80145-44-4
1-(2-furyl)-1-ethanone

: 1045704-66-2
2-(2-aminophenyl)-5-ethylfuran

Guidance literature:: Multi-step reaction with 3 steps

1.1: HCl / H₂O / 0.5 h / 80 °C

1.2: NaNO₂ / H₂O / 0.67 h / -10 - 0 °C

1.3: 41 percent / CuCl₂ / acetone; H₂O / 12 h / 20 °C

2.1: AlCl₃; NaBH₄ / tetrahydrofuran / Heating

3.1: hydrazin hydrate / Raney nickel / ethanol / Heating

With hydrogenchloride; sodium tetrahydroborate; aluminium trichloride; hydrazine hydrate; nickel; In tetrahydrofuran; ethanol; water; 1.1: Meerwein method;
DOI:10.1016/j.tetlet.2006.04.080