phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

Base Information

Chemical Name:phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside
CAS No.:1192142-77-0
Molecular Formula:C₉₀H₉₂Cl₃NO₁₆S
Molecular Weight:1582.14
Hs Code.:

phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

Synonyms:phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

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Chemical Property of phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

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Technology Process of phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

There total 2 articles about phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1192142-69-0
2,3,4-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-D-glucopyranosyl (N-phenyl)-2,2,2-trifluoroacetimidate

: 127299-77-8
phenyl 3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 1192142-77-0
phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - -40 ℃; stereoselective reaction;
DOI:10.1016/j.tet.2009.07.080

Reference yield: 44.0%

: 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-D-glucopyranosyl fluoride

: 127299-77-8
phenyl 3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 1192142-77-0
phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

Guidance literature:: With zirconocene dichloride; silver perchlorate; In dichloromethane; at -20 ℃; for 0.5h; stereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.tet.2009.07.080

Reference yield: 88.0%

: 1192142-77-0
phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

: 1192142-81-6
phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

Guidance literature:: With acetic acid; zinc; In ethyl acetate; for 0.5h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.tet.2009.07.080