5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II)

Base Information

Chemical Name:5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II)
CAS No.:1373621-30-7
Molecular Formula:C₆₈H₇₂Br₄MgN₄O₄
Molecular Weight:1353.27
Hs Code.:

Synonyms:5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II)

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Chemical Property of 5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II)

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Technology Process of 5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II)

There total 4 articles about 5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin

: 7789-48-2
magnesium bromide

: 1373621-30-7
5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II)

Guidance literature:: 5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin; magnesium bromide; In dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere;

With triethylamine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

Reference yield: 96.0%

: 5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin

: 1373621-30-7
5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II)

Guidance literature:: With triethylamine; magnesium bromide; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c2cc30591g

Reference yield:

: C₆₈H₈₀Br₄N₄O₄

: 1373621-30-7
5,10,15,20-tetrakis[3-(6-bromohexyloxy)phenyl]porphyrin magnesium(II)

Guidance literature:: Multi-step reaction with 2 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 9 h / 20 °C / Inert atmosphere

2: triethylamine; magnesium bromide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; magnesium bromide; In dichloromethane;
DOI:10.1039/c2cc30591g