(2S,6R)-6-[{(benzyloxy)carbonyl}amino]-2-{(tert-butyloxycarbonyl)amino}heptanedioic acid

Base Information

Chemical Name:(2S,6R)-6-[{(benzyloxy)carbonyl}amino]-2-{(tert-butyloxycarbonyl)amino}heptanedioic acid
CAS No.:1104583-26-7
Molecular Formula:C₂₀H₂₈N₂O₈
Molecular Weight:424.451
Hs Code.:

Synonyms:(2S,6R)-6-[{(benzyloxy)carbonyl}amino]-2-{(tert-butyloxycarbonyl)amino}heptanedioic acid

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Chemical Property of (2S,6R)-6-[{(benzyloxy)carbonyl}amino]-2-{(tert-butyloxycarbonyl)amino}heptanedioic acid

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Technology Process of (2S,6R)-6-[{(benzyloxy)carbonyl}amino]-2-{(tert-butyloxycarbonyl)amino}heptanedioic acid

There total 4 articles about (2S,6R)-6-[{(benzyloxy)carbonyl}amino]-2-{(tert-butyloxycarbonyl)amino}heptanedioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: (2S,6R)-6-amino-2-{(tert-butyloxycarbonyl)amino}heptanedioic acid

: 1104583-26-7
(2S,6R)-6-[{(benzyloxy)carbonyl}amino]-2-{(tert-butyloxycarbonyl)amino}heptanedioic acid

Guidance literature:: With sodium carbonate; In 1,4-dioxane; water; at 0 - 20 ℃; for 6h;
DOI:10.1039/c5ob02145f

Reference yield:

: 91216-98-7
2,6-Bis-acetylamino-heptanedioic acid

: 1104583-26-7
(2S,6R)-6-[{(benzyloxy)carbonyl}amino]-2-{(tert-butyloxycarbonyl)amino}heptanedioic acid

Guidance literature:: Multi-step reaction with 3 steps

1: cobalt(II) chloride hexahydrate / aq. phosphate buffer / 120 h / 40 °C / Enzymatic reaction

2: cobalt(II) chloride hexahydrate / aq. phosphate buffer / 168 h / 40 °C / Enzymatic reaction

3: sodium carbonate / 1,4-dioxane; water / 6 h / 0 - 20 °C

With cobalt(II) chloride hexahydrate; sodium carbonate; In 1,4-dioxane; aq. phosphate buffer; water;
DOI:10.1039/c5ob02145f

Reference yield:

: (2S,6R)-6-acetamido-2-((tert-butyloxycarbonyl)amino)heptanedioic acid

: 1104583-26-7
(2S,6R)-6-[{(benzyloxy)carbonyl}amino]-2-{(tert-butyloxycarbonyl)amino}heptanedioic acid

Guidance literature:: Multi-step reaction with 2 steps

1: cobalt(II) chloride hexahydrate / aq. phosphate buffer / 168 h / 40 °C / Enzymatic reaction

2: sodium carbonate / 1,4-dioxane; water / 6 h / 0 - 20 °C

With cobalt(II) chloride hexahydrate; sodium carbonate; In 1,4-dioxane; aq. phosphate buffer; water;
DOI:10.1039/c5ob02145f