Technology Process of C29H27NO5S
There total 3 articles about C29H27NO5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
AK lipase;
In
aq. phosphate buffer; acetone;
at 20 ℃;
for 15h;
pH=7;
Enzymatic reaction;
DOI:10.1016/j.bmcl.2012.11.010
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; dmap / dichloromethane / 0 °C
2: AK lipase / aq. phosphate buffer; acetone / 15 h / 20 °C / pH 7 / Enzymatic reaction
With
dmap; AK lipase; triethylamine;
In
aq. phosphate buffer; dichloromethane; acetone;
DOI:10.1016/j.bmcl.2012.11.010
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate; methanol / tetrahydrofuran / Reflux
2: triethylamine; dmap / dichloromethane / 0 °C
3: AK lipase / aq. phosphate buffer; acetone / 15 h / 20 °C / pH 7 / Enzymatic reaction
With
methanol; dmap; sodium tetrahydroborate; AK lipase; triethylamine;
In
tetrahydrofuran; aq. phosphate buffer; dichloromethane; acetone;
DOI:10.1016/j.bmcl.2012.11.010