4,4'-bis1-(3''-amino-4''-chlorophenyl)amidino>diphenylamine

Base Information

Chemical Name:4,4'-bis1-(3''-amino-4''-chlorophenyl)amidino>diphenylamine
CAS No.:82086-88-2
Molecular Formula:C₂₆H₂₃Cl₂N₇
Molecular Weight:504.422
Hs Code.:

4,4'-bis<N<sub>1</sub>-(3''-amino-4''-chlorophenyl)amidino>diphenylamine

Synonyms:4,4'-bis1-(3''-amino-4''-chlorophenyl)amidino>diphenylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-bis1-(3''-amino-4''-chlorophenyl)amidino>diphenylamine

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Technology Process of 4,4'-bis1-(3''-amino-4''-chlorophenyl)amidino>diphenylamine

There total 4 articles about 4,4'-bis1-(3''-amino-4''-chlorophenyl)amidino>diphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 82086-86-0
4,4'-Bis(4''-chloro-3''-nitroanilinoiminomethyl)diphenylamine

: 82086-88-2
4,4'-bis1-(3''-amino-4''-chlorophenyl)amidino>diphenylamine

Guidance literature:: With hydrogen; nickel; In tetrahydrofuran; for 14h; under 1838.8 Torr;

Reference yield:

: 635-22-3
4-Chloro-3-nitroaniline

: 82086-88-2
4,4'-bis1-(3''-amino-4''-chlorophenyl)amidino>diphenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / sodium ethoxide / ethanol / 72 h / 5 °C

2: 72 percent / hydrogen, Raney nickel / tetrahydrofuran / 14 h / 1838.8 Torr

With hydrogen; sodium ethanolate; nickel; In tetrahydrofuran; ethanol;

Reference yield:

: 36602-05-8
4,4’-dicyanodipehnylamine

: 82086-88-2
4,4'-bis1-(3''-amino-4''-chlorophenyl)amidino>diphenylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / HCl / benzene / 1.) 0 deg C, 2.) room temperature, 2 days

2: 86 percent / potassium carbonate / diethyl ether; H₂O

3: 67 percent / sodium ethoxide / ethanol / 72 h / 5 °C

4: 72 percent / hydrogen, Raney nickel / tetrahydrofuran / 14 h / 1838.8 Torr

With hydrogenchloride; hydrogen; sodium ethanolate; nickel; potassium carbonate; In tetrahydrofuran; diethyl ether; ethanol; water; benzene;