[Au^I(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl-AuCl₂-Au(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl]AuCl₄

Base Information

• Chemical Name: [Au^I(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl-AuCl₂-Au(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl]AuCl₄
• CAS No.: 1610951-64-8
• Molecular Formula: AuCl₄*C₃₄H₃₆Au₃Cl₄N₄P₂
• Molecular Weight: 1634.12

Synonyms:[Au^I(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl-AuCl₂-Au(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl]AuCl₄

Chemical Property of [Au^I(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl-AuCl₂-Au(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl]AuCl₄

Chemical Property:

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Technology Process of [Au^I(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl-AuCl₂-Au(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl]AuCl₄

There total 3 articles about [Au^I(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl-AuCl₂-Au(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl]AuCl₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

(1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) tetrachloroaurate (1610951-44-4) → [AuI(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl-AuCl2-Au(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl]AuCl4 (1610951-64-8)

Guidance literature:

In acetone; at 20 ℃; for 72h;

DOI:10.1016/j.jorganchem.2014.04.005

Reference yield:

chloro-diphenylphosphine (1079-66-9,74391-44-9) → [AuI(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl-AuCl2-Au(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl]AuCl4 (1610951-64-8)

Guidance literature:

Multi-step reaction with 4 steps

1: n-butyllithium / tetrahydrofuran; hexane / 4 h / -78 - 20 °C / Inert atmosphere

2: dichloromethane / 1 h / -78 °C / Inert atmosphere

3: dichloromethane

4: acetone / 72 h / 20 °C

With n-butyllithium; In tetrahydrofuran; hexane; dichloromethane; acetone;

DOI:10.1016/j.jorganchem.2014.04.005

Reference yield:

(1-methylimidazol-2-yl)diphenylphosphine (150404-18-5) → [AuI(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl-AuCl2-Au(1-methyl-2-diphenylphosphino-3-methylimidazolium)Cl]AuCl4 (1610951-64-8)

Guidance literature:

Multi-step reaction with 3 steps

1: dichloromethane / 1 h / -78 °C / Inert atmosphere

2: dichloromethane

3: acetone / 72 h / 20 °C

In dichloromethane; acetone;

DOI:10.1016/j.jorganchem.2014.04.005

upstream raw materials:

(1-methyl-2-diphenylphosphino-3-methylimidazolium)chlorogold(I) tetrachloroaurate

(1-methylimidazol-2-yl)diphenylphosphine

chloro-diphenylphosphine

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