CID 13621597

Base Information

Chemical Name:CID 13621597
CAS No.:102152-14-7
Molecular Formula:C₂₄H₃₁N₃O₅
Molecular Weight:441.527
Hs Code.:
ChEMBL ID:CHEMBL10825
DSSTox Substance ID:DTXSID701025200
Nikkaji Number:J1.550.928G

Synonyms:CHEMBL10825;102152-14-7;DTXSID701025200;BDBM50405414;1-[2-(3,4-dimethoxyphenyl)ethylamino]-3-[2-methoxy-4-(5-methyl-1H-imidazol-2-yl)phenoxy]propan-2-ol

Suppliers and Price of CID 13621597

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of CID 13621597

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:12
Exact Mass:441.22637110
Heavy Atom Count:32
Complexity:528

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CN=C(N1)C2=CC(=C(C=C2)OCC(CNCCC3=CC(=C(C=C3)OC)OC)O)OC

Technology Process of CID 13621597

There total 4 articles about CID 13621597 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102151-31-5
2-<4-(benzyloxy)-3-methoxyphenyl>-4-methylimidazole

: 102152-14-7
2-<3-methox-4-<3-<<2-(3,4-dimethopxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4-methylimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / H₂ / 10percent Pd/C / ethanol / 2585.7 Torr

2: 1.) NaH / 1.) DMF, 70 deg C, 15 min, 2.) DMF, 120 deg C, 18 h

3: H₂O, AcOH / 18 h / Ambient temperature

With water; hydrogen; sodium hydride; acetic acid; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00156a028

Reference yield:

: 3-[2-(3,4-Dimethoxy-phenyl)-ethyl]-5-[2-methoxy-4-(5-methyl-1H-imidazol-2-yl)-phenoxymethyl]-2-phenyl-oxazolidine

: 102152-14-7
2-<3-methox-4-<3-<<2-(3,4-dimethopxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4-methylimidazole

Guidance literature:: With water; acetic acid; for 18h; Yield given; Ambient temperature;
DOI:10.1021/jm00156a028

Reference yield:

: 85613-47-4,85613-59-8,91944-23-9
(S)-2-phenyl-3-<2-(3,4-dimethoxyphenyl)ethyl>-5-(hydroxymethyl)oxazolidine p-toluenesulfonate

: 102152-14-7
2-<3-methox-4-<3-<<2-(3,4-dimethopxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4-methylimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 70 deg C, 15 min, 2.) DMF, 120 deg C, 18 h

2: H₂O, AcOH / 18 h / Ambient temperature

With water; sodium hydride; acetic acid;
DOI:10.1021/jm00156a028