B/C-cis-4,9-dihydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridin

Base Information

• Chemical Name: B/C-cis-4,9-dihydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridin
• CAS No.: 101415-00-3
• Molecular Formula: C₁₉H₂₁NO₂
• Molecular Weight: 295.381

Synonyms:B/C-cis-4,9-dihydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridin

Chemical Property of B/C-cis-4,9-dihydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridin

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Technology Process of B/C-cis-4,9-dihydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridin

There total 2 articles about B/C-cis-4,9-dihydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

9-hydroxy-1-methyl-9-phenyl-1,2,3,4-tetrahydro-9H-indeno<2,1-b>pyridin-4-one (101414-94-2) → B/C-cis-4,9-dihydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridin (101415-00-3)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol;

DOI:10.1248/cpb.33.3287

Reference yield:

1-methyl-9-phenyl-1,2,3,4-tetrahydro-9H-indeno<2,1-b>pyridin-4-one (57420-18-5) → B/C-cis-4,9-dihydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridin (101415-00-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / KOH / propan-1-ol / 10 h / Heating

2: 94 percent / H₂ / PtO₂ / ethanol

With potassium hydroxide; hydrogen; platinum(IV) oxide; In propan-1-ol; ethanol;

DOI:10.1248/cpb.33.3287

Reference yield: 83.0%

acetic anhydride (108-24-7) + B/C-cis-4,9-dihydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridin (101415-00-3) → 4-acetoxy-9-hydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridine (101415-04-7)

Guidance literature:

With pyridine; at 40 ℃; for 48h;

DOI:10.1248/cpb.33.3287

upstream raw materials:

9-hydroxy-1-methyl-9-phenyl-1,2,3,4-tetrahydro-9H-indeno<2,1-b>pyridin-4-one

1-methyl-9-phenyl-1,2,3,4-tetrahydro-9H-indeno<2,1-b>pyridin-4-one

Downstream raw materials:

4-acetoxy-9-hydroxy-1-methyl-9-phenyl-1,2,3,4,4a,9a-hexahydro-9H-indeno<2,1-b>pyridine

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