benzyl 4-((2,4-bis(benzyloxy)-6-heptylbenzoyl)oxy)-2-heptyl-6-hydroxybenzoate

Base Information

Chemical Name:benzyl 4-((2,4-bis(benzyloxy)-6-heptylbenzoyl)oxy)-2-heptyl-6-hydroxybenzoate
CAS No.:1408253-09-7
Molecular Formula:C₄₉H₅₆O₇
Molecular Weight:756.979
Hs Code.:

Synonyms:benzyl 4-((2,4-bis(benzyloxy)-6-heptylbenzoyl)oxy)-2-heptyl-6-hydroxybenzoate

Suppliers and Price of benzyl 4-((2,4-bis(benzyloxy)-6-heptylbenzoyl)oxy)-2-heptyl-6-hydroxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 4-((2,4-bis(benzyloxy)-6-heptylbenzoyl)oxy)-2-heptyl-6-hydroxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 4-((2,4-bis(benzyloxy)-6-heptylbenzoyl)oxy)-2-heptyl-6-hydroxybenzoate

There total 4 articles about benzyl 4-((2,4-bis(benzyloxy)-6-heptylbenzoyl)oxy)-2-heptyl-6-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1408253-08-6
2,4-bis(benzyloxy)-6-heptylbenzoic acid

: 94693-37-5
benzyl 2-heptyl-4,6-dihydroxybenzoate

: 1408253-09-7
benzyl 4-((2,4-bis(benzyloxy)-6-heptylbenzoyl)oxy)-2-heptyl-6-hydroxybenzoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.08.116

Reference yield:

: 137571-76-7
7-(benzyloxy)-5-(hept-1-yn-1-yl)-2,2-dimethyl-4H-benzo[d][1,3]dioxin-4-one

: 1408253-09-7
benzyl 4-((2,4-bis(benzyloxy)-6-heptylbenzoyl)oxy)-2-heptyl-6-hydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol / 12 h / 760.05 Torr

2: tetrahydrofuran; dichloromethane / 72 h / Reflux

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / Inert atmosphere

With dmap; 10 wt% Pd(OH)2 on carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.08.116

Reference yield:

: 137571-77-8
2,2-dimethyl-5-(1-heptyl)-7-hydroxy-4H-1,3-benzodioxin-4-one

: 1408253-09-7
benzyl 4-((2,4-bis(benzyloxy)-6-heptylbenzoyl)oxy)-2-heptyl-6-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; dichloromethane / 72 h / Reflux

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / Inert atmosphere

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.08.116