2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4)-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4)-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside
CAS No.:1340668-12-3
Molecular Formula:C₃₇H₄₂N₄O₁₆
Molecular Weight:798.758
Hs Code.:

Synonyms:2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4)-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside

Suppliers and Price of 2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4)-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4)-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4)-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside

There total 2 articles about 2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4)-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1340668-11-2
2-azidoethyl 2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside

: 74808-10-9,86520-63-0,87119-53-7,92052-29-4,121238-27-5,142831-80-9,127061-80-7
2,3,4,6-tetra-O-acetyl-D-galactopyranosyl trichloroacetimidate

: 1340668-12-3
2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4)-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside

: C₅₁H₆₀N₄O₂₅

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; Inert atmosphere; Cooling;
DOI:10.1039/c1cc13310a

Reference yield:

: 169151-52-4
2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

: 1340668-12-3
2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4)-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: triethylsilane; trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / Inert atmosphere; Cooling

With triethylsilane; trimethylsilyl trifluoromethanesulfonate; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/c1cc13310a

Reference yield: 91.0%

: phenyl 3,4-di-O-acetyl-2-O-benzyl-1-thio-β-L-fucopyranoside

: 1340668-12-3
2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4)-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside

: 1340668-13-4
2-azidoethyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl(1->4) {2-O-benzyl-3,4-di-O-acetyl-α-L-fucosyl-(1->3)}-2-deoxy-2-phthalimidyl-6-O-benzyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 - 0 ℃; for 6h; Molecular sieve; Inert atmosphere;
DOI:10.1039/c1cc13310a