3,3,6,6?tetramethyl?9?(4?nitrophenyl)?10?(4?chlorophenyl)?1,8?dioxodecahydroacridine

Base Information

• Chemical Name: 3,3,6,6?tetramethyl?9?(4?nitrophenyl)?10?(4?chlorophenyl)?1,8?dioxodecahydroacridine
• CAS No.: 159301-99-2
• Molecular Formula: C₂₉H₂₉ClN₂O₄
• Molecular Weight: 505.013
• Mol file: 159301-99-2.mol

Synonyms:3,3,6,6?tetramethyl?9?(4?nitrophenyl)?10?(4?chlorophenyl)?1,8?dioxodecahydroacridine

Chemical Property of 3,3,6,6?tetramethyl?9?(4?nitrophenyl)?10?(4?chlorophenyl)?1,8?dioxodecahydroacridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3,6,6?tetramethyl?9?(4?nitrophenyl)?10?(4?chlorophenyl)?1,8?dioxodecahydroacridine

There total 1 articles about 3,3,6,6?tetramethyl?9?(4?nitrophenyl)?10?(4?chlorophenyl)?1,8?dioxodecahydroacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-nitrobenzaldehdye (555-16-8) + 4-chloro-aniline (106-47-8) + dimedone (126-81-8) → 3,3,6,6?tetramethyl?9?(4?nitrophenyl)?10?(4?chlorophenyl)?1,8?dioxodecahydroacridine (159301-99-2)

Guidance literature:

With graphene oxide decorated with platinum nanoparticles; In N,N-dimethyl-formamide; at 75 ℃; for 1.25h;

DOI:10.1039/c5ra06441d

Reference yield: 84.0%

3,3,6,6?tetramethyl?9?(4?nitrophenyl)?10?(4?chlorophenyl)?1,8?dioxodecahydroacridine (159301-99-2) → 9-(4-aminophenyl)-10-(4-chlorophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro acridine-1,8(2H,5H)-dione

Guidance literature:

With sulfur; sodium sulfide; In ethanol; water;

DOI:10.1007/s00044-017-2088-2

Reference yield:

3,3,6,6?tetramethyl?9?(4?nitrophenyl)?10?(4?chlorophenyl)?1,8?dioxodecahydroacridine (159301-99-2) → N-(4-(10-(4-chlorophenyl)-3,3,6,6-tetramethyl-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydro acridin-9-yl)phenyl)benzenesulfonamide

Guidance literature:

Multi-step reaction with 2 steps

1: sodium sulfide; sulfur / ethanol; water

2: tetrahydrofuran / 12 h / Reflux

With sulfur; sodium sulfide; In tetrahydrofuran; ethanol; water;

DOI:10.1007/s00044-017-2088-2

upstream raw materials:

4-nitrobenzaldehdye

4-chloro-aniline

dimedone