dispiro[7-methyl-2,3-dihydro-4(1H)-phenanthrene-4,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-xanthene]]

Base Information

Chemical Name:dispiro[7-methyl-2,3-dihydro-4(1H)-phenanthrene-4,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-xanthene]]
CAS No.:1166397-94-9
Molecular Formula:C₃₆H₃₀OS
Molecular Weight:510.7
Hs Code.:

Synonyms:dispiro[7-methyl-2,3-dihydro-4(1H)-phenanthrene-4,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-xanthene]]

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Chemical Property of dispiro[7-methyl-2,3-dihydro-4(1H)-phenanthrene-4,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-xanthene]]

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Technology Process of dispiro[7-methyl-2,3-dihydro-4(1H)-phenanthrene-4,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-xanthene]]

There total 1 articles about dispiro[7-methyl-2,3-dihydro-4(1H)-phenanthrene-4,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-xanthene]] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 134653-60-4
C₁₅H₁₆N₂

: 1166397-97-2
2-(2,6-dimethylphenyl)-9H-xanthene-9-thione

: 1166397-94-9
dispiro[7-methyl-2,3-dihydro-4(1H)-phenanthrene-4,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-xanthene]]

Guidance literature:: C₁₅H₁₆N₂; With methanol; potassium hydroxide; magnesium sulfate; silver(l) oxide; In dichloromethane; at 0 ℃; Inert atmosphere;

2-(2,6-dimethylphenyl)-9H-xanthene-9-thione; In dichloromethane; at 0 - 20 ℃; for 6h;
DOI:10.1016/j.tet.2009.03.081