4-cyclohexyl-2,3-butadienal

Base Information

• Chemical Name: 4-cyclohexyl-2,3-butadienal
• CAS No.: 1103181-67-4
• Molecular Formula: C₁₀H₁₄O
• Molecular Weight: 150.221
• Mol file: 1103181-67-4.mol

Synonyms:4-cyclohexyl-2,3-butadienal

Chemical Property of 4-cyclohexyl-2,3-butadienal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-cyclohexyl-2,3-butadienal

There total 2 articles about 4-cyclohexyl-2,3-butadienal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-cyclohexylbuta-2,3-dien-1-ol (153489-62-4) → 4-cyclohexyl-2,3-butadienal (1103181-67-4)

Guidance literature:

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; copper(II) nitrate trihydrate; oxygen; In 1,2-dichloro-ethane; at 25 ℃; for 22h;

Reference yield: 51.0%

cyclohexylallene (5664-17-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 4-cyclohexyl-2,3-butadienal (1103181-67-4)

Guidance literature:

cyclohexylallene; With n-butyllithium; In tetrahydrofuran; hexane; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane;

DOI:10.1039/b812869c

Reference yield: 86.0%

4-cyclohexyl-2,3-butadienal (1103181-67-4) + allyl bromide (106-95-6) → 1-cyclohexyl-1,2,6-heptatrien-4-ol (1103181-87-8)

Guidance literature:

4-cyclohexyl-2,3-butadienal; With indium; ammonium chloride; In tetrahydrofuran; water;

allyl bromide; In tetrahydrofuran; water; at 20 ℃; for 26.3h;

DOI:10.1039/b812869c

upstream raw materials:

cyclohexylallene

N,N-dimethyl-formamide

4-cyclohexylbuta-2,3-dien-1-ol

Downstream raw materials:

1-cyclohexyl-1,2,6-heptatrien-4-ol