Technology Process of C13H16FNO2
There total 7 articles about C13H16FNO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C17H20FNO5;
With
hydrogen bromide; acetic acid;
In
dichloromethane;
at 0 - 20 ℃;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 ℃;
for 1.5h;
With
sodium hydroxide; water;
In
tetrahydrofuran;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogen / palladium over charcoal / methanol / 20 °C
2.1: methanol / 2 h / 20 °C
2.2: 20 °C
3.1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / 0 - 20 °C
4.1: water; trifluoroacetic acid / 3 h / 50 °C
4.2: 20 °C
5.1: hydrogen bromide; acetic acid / dichloromethane / 0 - 20 °C
5.2: 1.5 h / 0 °C
With
water; hydrogen bromide; hydrogen; acetic acid; trifluoroacetic acid; (bis-(2-methoxyethyl)amino)sulfur trufluoride;
palladium over charcoal;
In
methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogen / palladium 10% on activated carbon / methanol / 1 h
2.1: methanol / 2 h / 20 °C
2.2: 20 °C
3.1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / 0 - 20 °C
4.1: water; trifluoroacetic acid / 3 h / 50 °C
4.2: 20 °C
5.1: hydrogen bromide; acetic acid / dichloromethane / 0 - 20 °C
5.2: 1.5 h / 0 °C
With
water; hydrogen bromide; hydrogen; acetic acid; trifluoroacetic acid; (bis-(2-methoxyethyl)amino)sulfur trufluoride;
palladium 10% on activated carbon;
In
methanol; dichloromethane;
