4-(carbo-t-butoxymethyl)-11-(N-phenylacetamido)-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

Base Information

Chemical Name:4-(carbo-t-butoxymethyl)-11-(N-phenylacetamido)-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane
CAS No.:942300-98-3
Molecular Formula:C₂₆H₄₃N₅O₃
Molecular Weight:473.659
Hs Code.:

Synonyms:4-(carbo-t-butoxymethyl)-11-(N-phenylacetamido)-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

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Chemical Property of 4-(carbo-t-butoxymethyl)-11-(N-phenylacetamido)-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

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Technology Process of 4-(carbo-t-butoxymethyl)-11-(N-phenylacetamido)-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

There total 3 articles about 4-(carbo-t-butoxymethyl)-11-(N-phenylacetamido)-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 942300-94-9
1,4,8,11-tetraazabicyclo[6.6.2]hexadecane-4-methanecarboxylic acid tert-butyl ester

: 587-65-5
N-chloroacetyl-aniline

: 942300-98-3
4-(carbo-t-butoxymethyl)-11-(N-phenylacetamido)-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

Guidance literature:: With sodium carbonate; potassium iodide; In acetonitrile; at 20 ℃; for 14h;
DOI:10.1021/jm070204r

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 942300-98-3
4-(carbo-t-butoxymethyl)-11-(N-phenylacetamido)-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / Na₂CO₃ / acetonitrile / 14 h / 20 °C

2: 73 percent / Na₂CO₃; KI / acetonitrile / 14 h / 20 °C

With sodium carbonate; potassium iodide; In acetonitrile;
DOI:10.1021/jm070204r

Reference yield:

: 130701-19-8
1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

: 942300-98-3
4-(carbo-t-butoxymethyl)-11-(N-phenylacetamido)-1,4,8,11-tetraazabicyclo[6.6.2]hexadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / Na₂CO₃ / acetonitrile / 14 h / 20 °C

2: 73 percent / Na₂CO₃; KI / acetonitrile / 14 h / 20 °C

With sodium carbonate; potassium iodide; In acetonitrile;
DOI:10.1021/jm070204r