methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate

Base Information

Chemical Name:methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate
CAS No.:1416152-72-1
Molecular Formula:C₄₂H₄₅N₃O₁₂
Molecular Weight:783.832
Hs Code.:

Synonyms:methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate

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Chemical Property of methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate

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Technology Process of methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate

There total 1 articles about methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1416152-71-0
methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-4-O-trichloroacetyl-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate

: 1416152-72-1
methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate

Guidance literature:: With pyridine; In methanol; at 50 ℃; for 6h;
DOI:10.1021/ol303112y

Reference yield: 88.0%

: 1416152-72-1
methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate

: 1416152-76-5
C₄₉H₄₆Cl₃N₃O₁₂S

: 1416152-73-2
methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-4-O-trichloroacetyl-α-D-glucopyranosyl)-(1?4)-(2-O-benzoyl-3-O-benzyl-α-L-idopyranosyl) uronate)-(1?4)-(methyl (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate

Guidance literature:: methyl (methyl (2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1?4)-2-O-benzoyl-3-O-benzyl-α-L-idopyranoside) uronate; C₄₉H₄₆Cl₃N₃O₁₂S; With N-iodo-succinimide; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere; Molecular sieve;

With silver trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol303112y