phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside
CAS No.:1363661-32-8
Molecular Formula:C₃₀H₃₈O₁₆S
Molecular Weight:688.689
Hs Code.:

Synonyms:phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Suppliers and Price of phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

There total 8 articles about phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₃₇F₃O₁₇⁽¹⁸⁾OS₂

: 1363661-32-8
phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Guidance literature:: With 2,6-dimethylpyridine; water; In tetrahydrofuran; at 40 ℃; for 1h;
DOI:10.1021/ja208564y

Reference yield:

: 1363661-30-6
phenyl (2,6-di-O-acetyl-4-O-(18)O-acetyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

: 1363661-32-8
phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 4 h / 0 - 20 °C

2: 2,6-dimethylpyridine; water / tetrahydrofuran / 1 h / 40 °C

With pyridine; 2,6-dimethylpyridine; water; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja208564y

Reference yield:

: 1363661-24-8
phenyl (2,6-di-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

: 1363661-32-8
phenyl (2,3,6-tri-O-acetyl-β-D-(3-(18)O)galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / acetonitrile / 0.5 h / 20 °C

1.2: 1 h

2.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.5 h / -78 - 20 °C

3.1: sodium nitrite / N,N-dimethyl-formamide / 50 °C

4.1: pyridine / dichloromethane / 4 h / 0 - 20 °C

5.1: 2,6-dimethylpyridine; water / tetrahydrofuran / 1 h / 40 °C

With pyridine; 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride; water; toluene-4-sulfonic acid; sodium nitrite; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja208564y