Technology Process of C40H46N5O18PS
There total 8 articles about C40H46N5O18PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 100 percent / H2 / 10percent Pd-C / methanol
2: N,N'-dicyclohexylcarbodiimide / 4-(N,N-dimethylamino)pyridine / benzene
3: boron trifluoride etherate / acetonitrile / 0.5 h / 0 °C
4: 67 percent / DMAP / CH2Cl2
5: Et3N / CH2Cl2 / 0 °C
6: toluene / 80 - 90 °C / 1-3 hrs
With
dmap; boron trifluoride diethyl etherate; hydrogen; triethylamine; dicyclohexyl-carbodiimide;
dmap; palladium on activated charcoal;
In
methanol; dichloromethane; toluene; acetonitrile; benzene;
DOI:10.1016/S0040-4039(01)81292-2
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 91 percent / pyridinium p-toluenesulfonate / tetrahydrofuran; H2O / 0.5 h / Ambient temperature
2: 100 percent / H2 / 10percent Pd-C / methanol
3: N,N'-dicyclohexylcarbodiimide / 4-(N,N-dimethylamino)pyridine / benzene
4: boron trifluoride etherate / acetonitrile / 0.5 h / 0 °C
5: 67 percent / DMAP / CH2Cl2
6: Et3N / CH2Cl2 / 0 °C
7: toluene / 80 - 90 °C / 1-3 hrs
With
dmap; boron trifluoride diethyl etherate; hydrogen; triethylamine; dicyclohexyl-carbodiimide;
dmap; palladium on activated charcoal; pyridinium p-toluenesulfonate;
In
tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile; benzene;
DOI:10.1016/S0040-4039(01)81292-2
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N,N'-dicyclohexylcarbodiimide / 4-(N,N-dimethylamino)pyridine / benzene
2: boron trifluoride etherate / acetonitrile / 0.5 h / 0 °C
3: 67 percent / DMAP / CH2Cl2
4: Et3N / CH2Cl2 / 0 °C
5: toluene / 80 - 90 °C / 1-3 hrs
With
dmap; boron trifluoride diethyl etherate; triethylamine; dicyclohexyl-carbodiimide;
dmap;
In
dichloromethane; toluene; acetonitrile; benzene;
DOI:10.1016/S0040-4039(01)81292-2