tert-butyl (2-oxo-8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-1(2H)-yl)acetate

Base Information

Chemical Name:tert-butyl (2-oxo-8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-1(2H)-yl)acetate
CAS No.:1424985-14-7
Molecular Formula:C₂₁H₂₂N₂O₄
Molecular Weight:366.417
Hs Code.:

Synonyms:tert-butyl (2-oxo-8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-1(2H)-yl)acetate

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Chemical Property of tert-butyl (2-oxo-8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-1(2H)-yl)acetate

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Technology Process of tert-butyl (2-oxo-8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-1(2H)-yl)acetate

There total 1 articles about tert-butyl (2-oxo-8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-1(2H)-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1424985-12-5
8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-2(1H)-one

: 1424985-14-7
tert-butyl (2-oxo-8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-1(2H)-yl)acetate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2012.12.024

Reference yield: 100.0%

: 1424985-14-7
tert-butyl (2-oxo-8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-1(2H)-yl)acetate

: 863724-54-3
(2-oxo-8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-1(2H)-yl)acetic acid

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; acetic acid; at 65 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2012.12.024

Reference yield:

: 1424985-14-7
tert-butyl (2-oxo-8-phenyl-4,5-dihydroimidazo[1,5,4-de][1,4]benzoxazin-1(2H)-yl)acetate

: C₂₄H₂₁N₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane; acetic acid / 65 °C / Inert atmosphere

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 7 h / 20 °C / Inert atmosphere

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.12.024