2-chloro-6-methylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide

Base Information

Chemical Name:2-chloro-6-methylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide
CAS No.:135217-03-7
Molecular Formula:C₁₉H₂₆ClN₃O₂S
Molecular Weight:395.953
Hs Code.:

Synonyms:2-chloro-6-methylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide

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Chemical Property of 2-chloro-6-methylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide

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Technology Process of 2-chloro-6-methylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide

There total 4 articles about 2-chloro-6-methylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 18858-05-4
2-chloro-6-methylbenzenethiol

: 135217-01-5
1-neopentyl-2-tert-butyl-4-nitro-5-chloroimidazole

: 135217-03-7
2-chloro-6-methylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide

Guidance literature:: With ammonia; In ethanol; a) 50 deg C, b) room temp., 2 h;
DOI:10.1002/jhet.5570280307

Reference yield:

: 67867-46-3
N,N'-dineopentyloxamide

: 135217-03-7
2-chloro-6-methylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide

Guidance literature:: Multi-step reaction with 3 steps

1: 36 percent / PCl₅ / 13.5 h / Heating

2: 1) conc. HNO₃, 2) conc. H₂SO₄ / 1) H₂O, 70 deg C, 0.5 h, 2) 2 h, reflux

3: 38 percent / NH₃ / ethanol / a) 50 deg C, b) room temp., 2 h

With phosphorus pentachloride; sulfuric acid; ammonia; nitric acid; In ethanol;
DOI:10.1002/jhet.5570280307

Reference yield:

: 5813-64-9
2.2-dimethylpropylamine

: 135217-03-7
2-chloro-6-methylphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfide

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / ethanol / 2 - 8 °C

2: 36 percent / PCl₅ / 13.5 h / Heating

3: 1) conc. HNO₃, 2) conc. H₂SO₄ / 1) H₂O, 70 deg C, 0.5 h, 2) 2 h, reflux

4: 38 percent / NH₃ / ethanol / a) 50 deg C, b) room temp., 2 h

With phosphorus pentachloride; sulfuric acid; ammonia; nitric acid; In ethanol;
DOI:10.1002/jhet.5570280307