a-acetyl-b-iodo-c,ed-bis{(2-methoxyethyl)diphenylphosphane-P;O'P'}rhodium(III)-hexafluoroantimonate

Base Information

Chemical Name:a-acetyl-b-iodo-c,ed-bis{(2-methoxyethyl)diphenylphosphane-P;O'P'}rhodium(III)-hexafluoroantimonate
CAS No.:123881-13-0
Molecular Formula:C₃₂H₃₇IO₃P₂Rh*F₆Sb
Molecular Weight:997.142
Hs Code.:

Synonyms:a-acetyl-b-iodo-c,ed-bis{(2-methoxyethyl)diphenylphosphane-P;O'P'}rhodium(III)-hexafluoroantimonate

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Chemical Property of a-acetyl-b-iodo-c,ed-bis{(2-methoxyethyl)diphenylphosphane-P;O'P'}rhodium(III)-hexafluoroantimonate

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Technology Process of a-acetyl-b-iodo-c,ed-bis{(2-methoxyethyl)diphenylphosphane-P;O'P'}rhodium(III)-hexafluoroantimonate

There total 1 articles about a-acetyl-b-iodo-c,ed-bis{(2-methoxyethyl)diphenylphosphane-P;O'P'}rhodium(III)-hexafluoroantimonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 123881-07-2
carbonyl-trans-bis{(2-methoxyethyl)diphenylphosphane-P;O',P'}rhodium(I)-hexafluoroantimonate

: 123881-13-0
a-acetyl-b-iodo-c,ed-bis{(2-methoxyethyl)diphenylphosphane-P;O'P'}rhodium(III)-hexafluoroantimonate

Guidance literature:: With methyl iodide; In tetrahydrofuran; all manipulations under Ar or N2; stirring soln. of Rh complex and CH3I in THF (20°C, 3 h); evapg., washing residue (2x, pentane); elem. anal.;

Reference yield:

: 123881-13-0
a-acetyl-b-iodo-c,ed-bis{(2-methoxyethyl)diphenylphosphane-P;O'P'}rhodium(III)-hexafluoroantimonate

: 123881-03-8
tricarbonyl-trans-bis{(2-methoxyethyl)diphenylphosphane}rhodium(I)-hexafluoroantimonate

Guidance literature:: With carbon monoxide; water; In tetrahydrofuran; water; byproducts: CH3COOH; stirring Rh complex in THF and H2O under CO gas (20°C, 30 min); detected by (31)P NMR and GC-MS;