tert-butyl 4--3-(2,6-dichlorophenyl)butyrate

Base Information

Chemical Name:tert-butyl 4--3-(2,6-dichlorophenyl)butyrate
CAS No.:132205-70-0
Molecular Formula:C₁₉H₂₇Cl₂NO₄
Molecular Weight:404.334
Hs Code.:

tert-butyl 4-<N-(tert-butoxycarbonyl)amino>-3-(2,6-dichlorophenyl)butyrate

Synonyms:tert-butyl 4--3-(2,6-dichlorophenyl)butyrate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 4--3-(2,6-dichlorophenyl)butyrate

Chemical Property:

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Technology Process of tert-butyl 4--3-(2,6-dichlorophenyl)butyrate

There total 4 articles about tert-butyl 4--3-(2,6-dichlorophenyl)butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 132205-70-0
tert-butyl 4--3-(2,6-dichlorophenyl)butyrate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA, 2.) HMPA / 1.) THF, -78 deg C, 30 min, 2.) THF, from -78 deg C to RT, 3 h

2: H₂ / PtO₂ / acetic acid / 1 h / 3102.9 Torr

3: aq. NaOH / tetrahydrofuran

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; hydrogen; lithium diisopropyl amide; platinum(IV) oxide; In tetrahydrofuran; acetic acid;
DOI:10.1021/jm00108a011

Reference yield:

: 3215-64-3
2,6-dichlorophenylacetonitrile

: 132205-70-0
tert-butyl 4--3-(2,6-dichlorophenyl)butyrate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA, 2.) HMPA / 1.) THF, -78 deg C, 30 min, 2.) THF, from -78 deg C to RT, 3 h

2: H₂ / PtO₂ / acetic acid / 1 h / 3102.9 Torr

3: aq. NaOH / tetrahydrofuran

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; hydrogen; lithium diisopropyl amide; platinum(IV) oxide; In tetrahydrofuran; acetic acid;
DOI:10.1021/jm00108a011

Reference yield:

: 132205-68-6
(+/-)-tert-butyl 3-cyano-3-(2,6-dichlorophenyl)propanoate

: 132205-70-0
tert-butyl 4--3-(2,6-dichlorophenyl)butyrate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / acetic acid / 1 h / 3102.9 Torr

2: aq. NaOH / tetrahydrofuran

With sodium hydroxide; hydrogen; platinum(IV) oxide; In tetrahydrofuran; acetic acid;
DOI:10.1021/jm00108a011