1,3-di(2-anisidyl)-3,4,5,6-tetrahydro-3H-[1,3]pyrimidinium tetrafluoroborate

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Chemical Name:1,3-di(2-anisidyl)-3,4,5,6-tetrahydro-3H-[1,3]pyrimidinium tetrafluoroborate
CAS No.:1192371-12-2
Molecular Formula:BF₄*C₁₈H₂₁N₂O₂
Molecular Weight:384.182
Hs Code.:

Synonyms:1,3-di(2-anisidyl)-3,4,5,6-tetrahydro-3H-[1,3]pyrimidinium tetrafluoroborate

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Chemical Property of 1,3-di(2-anisidyl)-3,4,5,6-tetrahydro-3H-[1,3]pyrimidinium tetrafluoroborate

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Technology Process of 1,3-di(2-anisidyl)-3,4,5,6-tetrahydro-3H-[1,3]pyrimidinium tetrafluoroborate

There total 1 articles about 1,3-di(2-anisidyl)-3,4,5,6-tetrahydro-3H-[1,3]pyrimidinium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1192371-33-7
1,3-di(2-anisidyl)-3,4,5,6-tetrahydro-3H-[1,3]pyrimidinium bromide

: 1192371-12-2
1,3-di(2-anisidyl)-3,4,5,6-tetrahydro-3H-[1,3]pyrimidinium tetrafluoroborate

Guidance literature:: With sodium tetrafluoroborate; In water; acetonitrile; Inert atmosphere;
DOI:10.1039/b909834h

Reference yield: 64.0%

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: 1192371-12-2
1,3-di(2-anisidyl)-3,4,5,6-tetrahydro-3H-[1,3]pyrimidinium tetrafluoroborate

: Rh(C₄H₆N₂(C₆H₄OCH₃)2)(C₈H₁₂)Cl

Guidance literature:: With KN(Si(CH₃)3)2; In tetrahydrofuran; under Ar; THF added to mixt. of KN(SiMe3)2 and BF4 salt of ligand; stirred for 30 min; filtered to THF soln. of Rh complex; stirred at room temp. for 2 h; volatiles removed in vac.; solid washed with hexane; dried; elem. anal.;
DOI:10.1039/b909834h