2,4-dimethoxy-3,5,6-trimethylbenzoic acid

Base Information

Chemical Name:2,4-dimethoxy-3,5,6-trimethylbenzoic acid
CAS No.:148238-84-0
Molecular Formula:C₁₂H₁₆O₄
Molecular Weight:224.257
Hs Code.:

Synonyms:2,4-dimethoxy-3,5,6-trimethylbenzoic acid

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Chemical Property of 2,4-dimethoxy-3,5,6-trimethylbenzoic acid

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Technology Process of 2,4-dimethoxy-3,5,6-trimethylbenzoic acid

There total 3 articles about 2,4-dimethoxy-3,5,6-trimethylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 148238-87-3
ethyl 2,4-dimethoxy-3,5,6-trimethylbenzoate

: 148238-84-0
2,4-dimethoxy-3,5,6-trimethylbenzoic acid

Guidance literature:: With potassium hydroxide; water; In dimethyl sulfoxide; at 90 - 95 ℃; for 4h;

Reference yield:

: 148238-89-5
ethyl 3-formyl-4,6-dihydroxy-2,5-dimethylbenzoate

: 148238-84-0
2,4-dimethoxy-3,5,6-trimethylbenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / glacial acetic acid, H₂ / 10percent Pd/C / ethyl acetate / 70 h / 45 °C

2: 98 percent / potassium carbonate / acetone / 22 h / Heating

3: 46 percent / potassium hydroxide, H₂O / dimethylsulfoxide / 4 h / 90 - 95 °C

With potassium hydroxide; water; hydrogen; potassium carbonate; acetic acid; palladium on activated charcoal; In dimethyl sulfoxide; ethyl acetate; acetone;

Reference yield:

: 81345-10-0
ethyl 2,4-dihydroxy-3,5,6-trimethylbenzoate

: 148238-84-0
2,4-dimethoxy-3,5,6-trimethylbenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / potassium carbonate / acetone / 22 h / Heating

2: 46 percent / potassium hydroxide, H₂O / dimethylsulfoxide / 4 h / 90 - 95 °C

With potassium hydroxide; water; potassium carbonate; In dimethyl sulfoxide; acetone;