N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside

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Chemical Name:N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside
CAS No.:1421768-02-6
Molecular Formula:C₁₀₇H₁₂₀BrNO₁₉Si
Molecular Weight:1832.11
Hs Code.:

N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside

Synonyms:N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside

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Chemical Property of N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside

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Technology Process of N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside

There total 1 articles about N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1421767-99-8
(2-methyl-5-tert-butylphenyl) 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-1-thio-β-D-glucopyranoside

: 1421768-01-5
N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside

: 1421768-02-6
N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -30 - -17 ℃; for 1h; Inert atmosphere; Molecular sieve;

Reference yield:

: 1421768-02-6
N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside

: 1421768-03-7
N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside; With potassium phosphate; tetrabutylammomium bromide; palladium diacetate; 3,4-Dimethoxyphenylboronic acid; In ethanol; for 2h; Inert atmosphere;

With sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; for 16h; Inert atmosphere;

With tetrabutyl ammonium fluoride; acetic acid; In N,N-dimethyl-formamide; at 50 ℃; for 72h; Inert atmosphere;

Reference yield:

: 1421768-02-6
N-(benzyl)benzyloxycarbonyl-5-aminopentanyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→4)-2,6-di-O-benzyl-3-O-(4-bromobenzyl)-α-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-α-D-glucopyranoside

: 122775-35-3
3,4-Dimethoxyphenylboronic acid

: C₁₁₅H₁₂₉NO₂₁Si

Guidance literature:: With potassium phosphate; tetrabutylammomium bromide; palladium diacetate; In ethanol; for 2h; Inert atmosphere;
DOI:10.1021/ja401410y