Technology Process of C24H29NO7
There total 1 articles about C24H29NO7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sulfuric acid / methanol / 30 h / 20 °C / Inert atmosphere
2: (1S)-10-camphorsulfonic acid / toluene / 5 h / Reflux; Inert atmosphere
With
sulfuric acid; (1S)-10-camphorsulfonic acid;
In
methanol; toluene;
DOI:10.1021/jo500493c
- Guidance literature:
-
With
lithium hydroxide monohydrate; water;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/jo500493c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C / Inert atmosphere
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
With
lithium hydroxide monohydrate; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo500493c