N-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl]cyclohexanecarboxamide

Base Information

Chemical Name:N-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl]cyclohexanecarboxamide
CAS No.:635302-12-4
Molecular Formula:C₆₅H₇₉NO₂₂
Molecular Weight:1226.34
Hs Code.:

N-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl]cyclohexanecarboxamide

Synonyms:N-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl]cyclohexanecarboxamide

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Chemical Property of N-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl]cyclohexanecarboxamide

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Technology Process of N-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl]cyclohexanecarboxamide

There total 1 articles about N-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl]cyclohexanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2719-27-9
cyclohexanylcarbonyl chloride

: acetic acid 5-acetoxy-6-acetoxymethyl-2-(4,5-diacetoxy-2-acetoxymethyl-6-amino-tetrahydro-pyran-3-yloxy)-4-(3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

: 635302-12-4
N-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl]cyclohexanecarboxamide

Guidance literature:: With triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1081/CAR-120025323

Reference yield:

: 635302-12-4
N-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl]cyclohexanecarboxamide

: acetic acid 5-acetoxy-6-acetoxymethyl-2-[4,5-diacetoxy-2-acetoxymethyl-6-(cyclohexanecarbonyl-amino)-tetrahydro-pyran-3-yloxy]-4-(3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 5h; under 2585.74 Torr;
DOI:10.1081/CAR-120025323

Reference yield:

: 635302-12-4
N-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl]cyclohexanecarboxamide

: N-[O-α-D-galactopyranosyl-(1->3)-O-β-D-galactopyranosyl-(1->4)-1-β-D-glucopyranosyl]cyclohexanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol / 5 h / 2585.74 Torr

2: NaOMe / methanol / 2 h

With hydrogen; sodium methylate; palladium on activated charcoal; In methanol;
DOI:10.1081/CAR-120025323