C₄₃H₆₀O₁₀Si

Base Information

Chemical Name:C₄₃H₆₀O₁₀Si
CAS No.:153145-49-4
Molecular Formula:C₄₃H₆₀O₁₀Si
Molecular Weight:765.029
Hs Code.:

C<sub>43</sub>H<sub>60</sub>O<sub>10</sub>Si

Synonyms:C₄₃H₆₀O₁₀Si

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Chemical Property of C₄₃H₆₀O₁₀Si

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Technology Process of C₄₃H₆₀O₁₀Si

There total 21 articles about C₄₃H₆₀O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153145-26-7
C₃₂H₅₆O₇Si₂

: 153145-49-4
C₄₃H₆₀O₁₀Si

Guidance literature:: Multi-step reaction with 10 steps

1: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

2: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

3: 95 percent / CH₂Cl₂ / 15 h / -45 °C

4: 63 percent / Burgess' reagent

5: 100 percent / pyridine

6: 65 percent / OsO₄

7: DBU / toluene / 2 h / 105 °C

8: 75 percent / pyridine, DMAP / 24 h / 25 °C

9: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

10: tetrahydrofuran / 0.17 h / -78 °C

With pyridine; dmap; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

: 153145-49-4
C₄₃H₆₀O₁₀Si

Guidance literature:: Multi-step reaction with 17 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

11: 63 percent / Burgess' reagent

12: 100 percent / pyridine

13: 65 percent / OsO₄

14: DBU / toluene / 2 h / 105 °C

15: 75 percent / pyridine, DMAP / 24 h / 25 °C

16: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

17: tetrahydrofuran / 0.17 h / -78 °C

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; pyridine hydrogenfluoride; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 153145-25-6
C₃₆H₆₄O₈Si₂

: 153145-49-4
C₄₃H₆₀O₁₀Si

Guidance literature:: Multi-step reaction with 11 steps

1: acid

2: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

3: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

4: 95 percent / CH₂Cl₂ / 15 h / -45 °C

5: 63 percent / Burgess' reagent

6: 100 percent / pyridine

7: 65 percent / OsO₄

8: DBU / toluene / 2 h / 105 °C

9: 75 percent / pyridine, DMAP / 24 h / 25 °C

10: 100 percent / HF*pyridine / acetonitrile / 11 h / 0 °C

11: tetrahydrofuran / 0.17 h / -78 °C

With pyridine; dmap; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; pyridine hydrogenfluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;