1,3-Dioxolane, 2,2,4-trimethyl-5-(phenylmethoxy)methyl-, cis-

Base Information

Chemical Name:1,3-Dioxolane, 2,2,4-trimethyl-5-(phenylmethoxy)methyl-, cis-
CAS No.:124019-21-2
Molecular Formula:C₁₄H₂₀O₃
Molecular Weight:236.311
Hs Code.:
Mol file:124019-21-2.mol

Synonyms:1,3-Dioxolane,2,2,4-trimethyl-5-[(phenylmethoxy)methyl]-, cis- (9CI); 1,3-Dioxolane, 2,2,4-trimethyl-5-[(phenylmethoxy)methyl]-,cis-(?à)-

Suppliers and Price of 1,3-Dioxolane, 2,2,4-trimethyl-5-(phenylmethoxy)methyl-, cis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 1,3-Dioxolane, 2,2,4-trimethyl-5-(phenylmethoxy)methyl-, cis-

Chemical Property:

PSA：27.69000
LogP:2.74320

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-Dioxolane, 2,2,4-trimethyl-5-(phenylmethoxy)methyl-, cis-

There total 7 articles about 1,3-Dioxolane, 2,2,4-trimethyl-5-(phenylmethoxy)methyl-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 78513-04-9
(4S,5S)-p-toluolsulfonsaeure<(5-benzyloxymethyl-5-hydroxymethyl-2,2-dimethyl-1,3-dioxolan-4-yl)methyl>ester

: 85099-89-4,109715-57-3,124019-21-2,93451-86-6
(S,S)-2,2-dimethyl-4-benzyloxymethyl-5-methyl-1,3-dioxolane

Guidance literature:: With sodium tetrahydroborate; In dimethyl sulfoxide; at 50 ℃; for 13h;
DOI:10.1248/cpb.37.1446

Reference yield: 92.0%

: 114826-50-5
(4R,5S)-2,2-dimethyl-4-iodomethyl-5-benzyloxymethyl-1,3-dioxolane

: 85099-89-4,109715-57-3,124019-21-2,93451-86-6
(S,S)-2,2-dimethyl-4-benzyloxymethyl-5-methyl-1,3-dioxolane

Guidance literature:: With 20 % Pd(OH)2/C; hydrogen; triethylamine; In methanol; at 20 ℃; for 24h; under 760.051 Torr; optical yield given as %de;
DOI:10.1039/c2ob25099c

Reference yield:

: 50622-09-8
2,3-O-isopropylidene-L-threitol

: 85099-89-4,109715-57-3,124019-21-2,93451-86-6
(S,S)-2,2-dimethyl-4-benzyloxymethyl-5-methyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide

2: pyridine

3: NaBH₄

With pyridine; sodium tetrahydroborate; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)95946-X