2,2,11,11-tetraphenyl-1,5,8,12-tetrathiadodecane

Base Information

• Chemical Name: 2,2,11,11-tetraphenyl-1,5,8,12-tetrathiadodecane
• CAS No.: 153335-66-1
• Molecular Formula: C₃₂H₃₄S₄
• Molecular Weight: 546.886

Synonyms:2,2,11,11-tetraphenyl-1,5,8,12-tetrathiadodecane

Chemical Property of 2,2,11,11-tetraphenyl-1,5,8,12-tetrathiadodecane

Chemical Property:

Purity/Quality:

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Technology Process of 2,2,11,11-tetraphenyl-1,5,8,12-tetrathiadodecane

There total 2 articles about 2,2,11,11-tetraphenyl-1,5,8,12-tetrathiadodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C42H50O2S4 → 2,2,11,11-tetraphenyl-1,5,8,12-tetrathiadodecane (153335-66-1)

Guidance literature:

With titanium tetrachloride; triethylamine; 2-hydroxyethanethiol; In dichloromethane; Ambient temperature;

DOI:10.1246/cl.1996.999

Reference yield:

C18H19LiOS → 2,2,11,11-tetraphenyl-1,5,8,12-tetrathiadodecane (153335-66-1)

Guidance literature:

Multi-step reaction with 2 steps

2: 97 percent / TiCl₄, Et₃N, HSCH₂CH₂OH / CH₂Cl₂ / Ambient temperature

With titanium tetrachloride; triethylamine; 2-hydroxyethanethiol; In dichloromethane;

DOI:10.1246/cl.1996.999

Reference yield: 75.5%

nickel(II) acetylacetonate dihydrate + 2,2,11,11-tetraphenyl-1,5,8,12-tetrathiadodecane (153335-66-1) → Ni((CH2SCH2CH2C(C6H5)2S)2)*2(CH3)2NCHO

Guidance literature:

In toluene; equimolar amts., stirring overnight (pptn.); collection (filtration), recrystn. (DMF, -15°C), collection (filtration), washing (ether), drying (vac.); elem. anal.;

DOI:10.1016/s0020-1693(97)05653-3

Downstream raw materials:

Ni(C₃₂H₃₂S₄)

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