N₁,N₇-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-4-nitroheptanediamide

Base Information

• Chemical Name: N₁,N₇-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-4-nitroheptanediamide
• CAS No.: 1260095-58-6
• Molecular Formula: C₄₀H₅₄N₄O₁₁
• Molecular Weight: 766.889

Synonyms:N₁,N₇-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-4-nitroheptanediamide

Chemical Property of N₁,N₇-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-4-nitroheptanediamide

Chemical Property:

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Technology Process of N₁,N₇-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-4-nitroheptanediamide

There total 1 articles about N₁,N₇-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-4-nitroheptanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(2-carboxyethyl)-4-nitroheptanedioic acid (59085-15-3) + 1,3-bis(methoxymethyl)aniline (1260095-54-2) → N1,N7-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-4-nitroheptanediamide (1260095-58-6)

Guidance literature:

4-(2-carboxyethyl)-4-nitroheptanedioic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

1,3-bis(methoxymethyl)aniline; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

DOI:10.1021/ja106076h

Reference yield: 90.0%

N1,N7-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-4-nitroheptanediamide (1260095-58-6) → 4-amino-N1,N7-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)heptanediamide (1260095-60-0)

Guidance literature:

With hydrogen; In ethanol; at 20 ℃; for 12h;

DOI:10.1021/ja106076h

Reference yield:

N1,N7-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-4-nitroheptanediamide (1260095-58-6) → 4-(2,2-diphenylbenzo[d][1,3]dioxole-5-carboxamido)-N1,N7-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)heptanediamide (1260095-64-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogen / ethanol / 12 h / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1 h / 0 °C

2.2: 48 h / 20 °C

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; N,N-dimethyl-formamide;

DOI:10.1021/ja106076h

upstream raw materials:

4-(2-carboxyethyl)-4-nitroheptanedioic acid

1,3-bis(methoxymethyl)aniline

Downstream raw materials:

4-amino-N₁,N₇-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)heptanediamide

4-(2,2-diphenylbenzo[d][1,3]dioxole-5-carboxamido)-N₁,N₇-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)heptanediamide

N₁,N₇-bis(3,5-bis(bromomethyl)phenyl)-4-(3-(3,5-bis(bromomethyl)phenylamino)-3-oxopropyl)-4-(3,4-dihydroxybenzamido)heptanediamide

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