Technology Process of C21H18O2
There total 5 articles about C21H18O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene;
In
tert-butyl alcohol;
at 20 ℃;
DOI:10.1016/j.tetlet.2011.12.118
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: methanesulfonyl chloride; triethylamine / dichloromethane / 3.17 h / 0 °C / Reflux
2.1: tert.-butyl lithium / tetrahydrofuran; hexane / 1.5 h / -78 - 20 °C
2.2: 1 h / 0 °C
2.3: Saturated solution
3.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tert-butyl alcohol / 20 °C
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; tert.-butyl lithium; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran; hexane; dichloromethane; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.12.118
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tert.-butyl lithium / tetrahydrofuran; hexane / 1.5 h / -78 - 20 °C
1.2: 1 h / 0 °C
1.3: Saturated solution
2.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tert-butyl alcohol / 20 °C
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; tert.-butyl lithium;
In
tetrahydrofuran; hexane; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.12.118
