Synonyms:Alnuserrutriol
There total 1 articles about 24-Methylene-3β,12β,20-dammaranetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
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The research focused on the isolation and structural elucidation of a new C20 dammarane-type triterpenoid, alnuserrutriol, derived from the male flowers of Alnus serrulatoides. The purpose of the study was to determine the chemical structure of alnuserrutriol using a combination of chemical and spectroscopic methods. The researchers concluded that alnuserrutriol has the structure (3S,12R,20S)-3,12,20-trihydroxy-24-methylenedammarane, which was confirmed by comparing its spectral data with that of a synthetic triol obtained by reducing alnuserrudiolone (II) with lithium aluminum hydride (LiAlH4). Key chemicals used in the process included acetone for extraction, ether for solubility testing, silica gel for chromatography, and hexane-EtOAc mixtures for TLC and centrifugal chromatography. The study also utilized various spectroscopic techniques such as infrared (IR), proton nuclear magnetic resonance (1H NMR), carbon-13 nuclear magnetic resonance (13C NMR), and mass spectrometry (MS) to analyze the compound's properties and confirm its structure.
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