4,4-Diethoxybut-2-yn-1-amine

Base Information

Chemical Name:4,4-Diethoxybut-2-yn-1-amine
CAS No.:124744-14-5
Molecular Formula:C8H15 N O2
Molecular Weight:157.2102
Hs Code.:
DSSTox Substance ID:DTXSID90369239
Wikidata:Q82156284
Mol file:124744-14-5.mol

Synonyms:4,4-diethoxybut-2-yn-1-amine;124744-14-5;4,4-DIETHOXY-BUT-2-YNYLAMINE;DTXSID90369239;AKOS006275458;AT19989;FT-0733591;EN300-7547805

Suppliers and Price of 4,4-Diethoxybut-2-yn-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4,4-DIETHOXY-BUT-2-YNYLAMINE 95.00%
5MG
$ 500.68

Total 2 raw suppliers

Chemical Property of 4,4-Diethoxybut-2-yn-1-amine

Chemical Property:

PSA：44.48000
LogP:1.04790
XLogP3:-0.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:157.110278721
Heavy Atom Count:11
Complexity:139

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

4,4-DIETHOXY-BUT-2-YNYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(C#CCN)OCC

Technology Process of 4,4-Diethoxybut-2-yn-1-amine

There total 4 articles about 4,4-Diethoxybut-2-yn-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16548-24-6
1,1-diethoxy-4-methanesulfonyloxy-but-2-yne

: 124744-14-5
4,4-Diethoxy-but-2-ynylamine

Guidance literature:: With ammonium hydroxide; at 20 ℃; for 1.5h; Yield given;
DOI:10.1016/S0040-4039(00)99296-7

Reference yield:

: 18350-44-2
4,4-diethoxy-but-2-yn-1-ol

: 124744-14-5
4,4-Diethoxy-but-2-ynylamine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / diethyl ether / 1 h / 0 °C

2: aq. NH₃ / 2.5 h / 20 °C

With ammonium hydroxide; triethylamine; In diethyl ether;
DOI:10.1021/jo048794d

Reference yield:

: 74149-25-0
4,4-diethoxy-2-butynal

: 124744-14-5
4,4-Diethoxy-but-2-ynylamine

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / methanol / 0 °C

2: Et₃N / CH₂Cl₂

3: aqueous NH₃ / 1.5 h / 20 °C

With ammonium hydroxide; sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(00)99296-7