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(2S,3R)-3-HYDROXY-L-ISOVALINE

Base Information Edit
  • Chemical Name:(2S,3R)-3-HYDROXY-L-ISOVALINE
  • CAS No.:127126-06-1
  • Molecular Formula:C5H11NO3
  • Molecular Weight:133.147
  • Hs Code.:
  • Mol file:127126-06-1.mol
(2S,3R)-3-HYDROXY-L-ISOVALINE

Synonyms:L-Isovaline,3-hydroxy-, (3R)- (9CI); L-Isovaline, 3-hydroxy-, (R)-

Suppliers and Price of (2S,3R)-3-HYDROXY-L-ISOVALINE
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • American Custom Chemicals Corporation
  • (2S,3R)-3-HYDROXY-L-ISOVALINE 95.00%
  • 5MG
  • $ 496.52
Total 4 raw suppliers
Chemical Property of (2S,3R)-3-HYDROXY-L-ISOVALINE Edit
Chemical Property:
  • Boiling Point:317.3±32.0 °C(Predicted) 
  • PKA:2.23±0.14(Predicted) 
  • PSA:83.55000 
  • Density:1.240±0.06 g/cm3(Predicted) 
  • LogP:-0.13050 
Purity/Quality:

97% *data from raw suppliers

(2S,3R)-3-HYDROXY-L-ISOVALINE 95.00% *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of (2S,3R)-3-HYDROXY-L-ISOVALINE

There total 13 articles about (2S,3R)-3-HYDROXY-L-ISOVALINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium hydroxide; In methanol; for 3h; Ambient temperature;
DOI:10.1021/jo971983u
Guidance literature:
methyl (2R,3S,7R,7aS)-7-methoxy-2,3,7,7a-tetramethyl-5-oxotetrahydro-2H-oxazolo[4,3-b]oxazole-3-carboxylate; With hydrogenchloride; In water; Reflux;
With methyloxirane; In ethanol; for 0.666667h; Reflux;
DOI:10.1016/j.tetasy.2008.11.031
Guidance literature:
Multi-step reaction with 6 steps
1: 85 percent / AD-mix β, methanesulfonamide / 2-methyl-propan-2-ol; H2O / 48 h / 4 °C
2: SOCl2 / CH2Cl2 / 2.5 h / 40 °C
3: 91 percent / NaIO4, RuCl3 hydrate / acetonitrile; CCl4; H2O / 3 h / 40 °C
4: 1.) NaN3, 2.) aq. H2SO4 / 1.) DMF, room temp., 4 h, then 50 deg C, 3 h, 2.) Et2O, 20 deg C, 48 h
5: 98 percent / H2 / Pd/C / methanol
6: 89.4 percent / aq. NaOH / methanol / 3 h / Ambient temperature
With ruthenium trichloride; sodium hydroxide; sodium periodate; thionyl chloride; sodium azide; methanesulfonamide; sulfuric acid; hydrogen; 1,4-bis(9-O-dihydroquinidine)phthalazine; palladium on activated charcoal; In methanol; tetrachloromethane; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jo971983u
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