3-Pyrazolidinone, 2-acetyl-4,5-dimethyl-, trans- (9CI)

Base Information

Chemical Name:3-Pyrazolidinone, 2-acetyl-4,5-dimethyl-, trans- (9CI)
CAS No.:130064-86-7
Molecular Formula:C₇H₁₂N₂O₂
Molecular Weight:156.184
Hs Code.:
Mol file:130064-86-7.mol

Synonyms:3-Pyrazolidinone,2-acetyl-4,5-dimethyl-, trans- (9CI); 3-Pyrazolidinone, 2-acetyl-4,5-dimethyl-,trans-(?à)-

Suppliers and Price of 3-Pyrazolidinone, 2-acetyl-4,5-dimethyl-, trans- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 3-Pyrazolidinone, 2-acetyl-4,5-dimethyl-, trans- (9CI)

Chemical Property:

PSA：49.41000
LogP:0.17100

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Pyrazolidinone, 2-acetyl-4,5-dimethyl-, trans- (9CI)

There total 4 articles about 3-Pyrazolidinone, 2-acetyl-4,5-dimethyl-, trans- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 130064-83-4,130064-84-5
2-Acetyl-4,5-dimethyl-1-(2,2,2-trichloroethoxycarboxyl)pyrazolidin-3-one

: 130064-85-6,130064-86-7
2-Acetyl-4,5-dimethylpyrazolidin-3-one

Guidance literature:: With zinc; In acetic acid; for 2h; Ambient temperature;
DOI:10.1021/jo00311a023

Reference yield:

: 80-59-1
Tiglic acid

: 130064-85-6,130064-86-7
2-Acetyl-4,5-dimethylpyrazolidin-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / hydrazine hydrate / neutral alumina / butan-1-ol; benzene / 94 - 95 °C

2: 57 percent / 2N NaOH / tetrahydrofuran / 3 h / Ambient temperature

3: 1) triethylamine / 1) THF, 0 deg C, 2) neat, 110 deg C

4: 60 percent / Zn dust / acetic acid / 2 h / Ambient temperature

With sodium hydroxide; hydrazine hydrate; triethylamine; zinc; aluminum oxide; In tetrahydrofuran; acetic acid; butan-1-ol; benzene;
DOI:10.1021/jo00311a023

Reference yield:

: 130064-78-7,130064-79-8
4,5-Dimethylpyrazolidin-3-one

: 130064-85-6,130064-86-7
2-Acetyl-4,5-dimethylpyrazolidin-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / 2N NaOH / tetrahydrofuran / 3 h / Ambient temperature

2: 1) triethylamine / 1) THF, 0 deg C, 2) neat, 110 deg C

3: 60 percent / Zn dust / acetic acid / 2 h / Ambient temperature

With sodium hydroxide; triethylamine; zinc; In tetrahydrofuran; acetic acid;
DOI:10.1021/jo00311a023