2-Cyclobuten-1-one, 4-hydroxy-2,3-dimethyl-4-(1-propynyl)- (9CI)

Base Information

Chemical Name:2-Cyclobuten-1-one, 4-hydroxy-2,3-dimethyl-4-(1-propynyl)- (9CI)
CAS No.:130352-47-5
Molecular Formula:C9H10 O2
Molecular Weight:150.1745
Hs Code.:
Mol file:130352-47-5.mol

Synonyms:2-Cyclobuten-1-one,4-hydroxy-2,3-dimethyl-4-(1-propynyl)- (9CI)

Suppliers and Price of 2-Cyclobuten-1-one, 4-hydroxy-2,3-dimethyl-4-(1-propynyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Cyclobuten-1-one, 4-hydroxy-2,3-dimethyl-4-(1-propynyl)- (9CI)

Chemical Property:

PSA：37.30000
LogP:0.65990

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Cyclobuten-1-one, 4-hydroxy-2,3-dimethyl-4-(1-propynyl)- (9CI)

There total 1 articles about 2-Cyclobuten-1-one, 4-hydroxy-2,3-dimethyl-4-(1-propynyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 36147-87-2
1-propynyl anion

: 1121-15-9
3,4-dimethylcyclobut-3-ene-1,2-dione

: 130352-47-5
4-C₂Me-4-hydroxy-3-methyl-2-methyl-2-cyclobuten-1-one

Guidance literature:: DOI:10.1021/ja00179a072

Reference yield: 78.0%

: 1067-52-3
tributyltin methoxide

: 130352-47-5
4-C₂Me-4-hydroxy-3-methyl-2-methyl-2-cyclobuten-1-one

: 130352-56-6
2,3,5-Trimethyl-6-(tri-n-butylstannyl)-1,4-benzoquinone

Guidance literature:: thermolysis of soln. of organic compound in dichloroethane in the presence of n-Bu3SnOMe for 10-15 min;
DOI:10.1021/ja00179a072

Reference yield:

: 130352-47-5
4-C₂Me-4-hydroxy-3-methyl-2-methyl-2-cyclobuten-1-one

: 2134-78-3
2,3,5-trimethyl-6-(3-methylbut-2-enyl)cyclohexa-2,5-diene-1,4-dione

Guidance literature:: With tributyltin methoxide; palladium; Yield given. Multistep reaction; 1.) dichloroethane, reflux;
DOI:10.1021/ja00179a072