L-SERYL-L-PHENYLALANINAMIDE HYDROCHLORIDE

Base Information

• Chemical Name: L-SERYL-L-PHENYLALANINAMIDE HYDROCHLORIDE
• CAS No.: 130816-88-5
• Molecular Formula: C12H17 N3 O3 . Cl H
• Molecular Weight: 0
• Hs Code.: 2924299090
• Mol file: 130816-88-5.mol

Synonyms:L-SERYL-L-PHENYLALANINAMIDE HYDROCHLORIDE

Chemical Property of L-SERYL-L-PHENYLALANINAMIDE HYDROCHLORIDE

Chemical Property:

• Melting Point: 204-205 °C
• PSA: 118.44000
• LogP: 1.11230

Purity/Quality:

99% ^*data from raw suppliers

H-Ser-Phe-NH2Hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of L-SERYL-L-PHENYLALANINAMIDE HYDROCHLORIDE

There total 4 articles about L-SERYL-L-PHENYLALANINAMIDE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Boc-Ser-Phe-NH2 (107897-21-2) → Ser-Phe-NH2 hydrochloride (130816-88-5)

Guidance literature:

With trifluoroacetic acid; at 0 ℃; for 1h;

DOI:10.1246/bcsj.63.1753

Reference yield:

(S)-2-amino-3-phenylpropionamide hydrochloride (65864-22-4) → Ser-Phe-NH2 hydrochloride (130816-88-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 64 percent / Et₃N, DCC, HOBt / dimethylformamide / 1) 0 deg C, 2) r.t., overnight

2: 95 percent / TFA / 1 h / 0 °C

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;

DOI:10.1246/bcsj.63.1753

Reference yield:

N-(N-benzyloxycarbonyl-L-seryl)-L-phenylalanine amide (25529-46-8) → Ser-Phe-NH2 hydrochloride (130816-88-5)

Guidance literature:

With hydrogenchloride; palladium; Hydrogenation;

upstream raw materials:

N-(N-benzyloxycarbonyl-L-seryl)-L-phenylalanine amide

Boc-Ser-Phe-NH₂

(S)-2-amino-3-phenylpropionamide hydrochloride

H-Phe-OEt

Downstream raw materials:

H-Tyr-Pro-Ser-Phe-NH₂*AcOH

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