Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-(acetylamino)-, (1S-endo)- (9CI)

Base Information

• Chemical Name: Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-(acetylamino)-, (1S-endo)- (9CI)
• CAS No.: 131177-83-8
• Molecular Formula: C₁₀H₁₃NO₃
• Molecular Weight: 195.218
• Mol file: 131177-83-8.mol

Synonyms:Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-(acetylamino)-, (1S-endo)- (9CI)

Chemical Property of Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-(acetylamino)-, (1S-endo)- (9CI)

Chemical Property:

• PSA: 66.40000
• LogP: 0.93280

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-(acetylamino)-, (1S-endo)- (9CI)

There total 11 articles about Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-(acetylamino)-, (1S-endo)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

methyl 2-endo-acetamidobicyclo<2.2.1>hept-5-ene-2-exo-carboxylate (72431-82-4,72431-85-7,131150-28-2,131150-29-3,136314-92-6,136314-93-7,139237-37-9,139237-38-0) → (1RS,2RS,4RS)-2-acetylamino-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid (131053-13-9,131102-02-8,131102-03-9,131177-83-8,133007-77-9,133007-78-0)

Guidance literature:

With potassium hydroxide; ethanol; at 110 ℃; for 2h;

DOI:10.1016/j.bmc.2007.09.004

Reference yield: 86.0%

methyl 2-exo-acetamidobicyclo<2.2.1>hept-5-ene-2-endo-carboxylate (72431-82-4,72431-85-7,131150-28-2,131150-29-3,136314-92-6,136314-93-7,139237-37-9,139237-38-0) → 2-exo-Acetamidonorbornene-2-endo-carboxylic acid (131053-13-9,131102-02-8,131102-03-9,131177-83-8,133007-77-9,133007-78-0)

Guidance literature:

With potassium hydroxide; ethanol; at 110 ℃; for 2h;

DOI:10.1016/j.bmc.2007.09.004

Reference yield: 79.0%

(1'R,3'R,4'S)-8'-phenylmenthyl (1S,2S,4S)-2-acetylamino-bicyclo[2.2.1]hept-5-ene-2-carboxylate (905733-12-2) → (1S,2S,4S)-(-)-2-acetylamino-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid (131177-83-8)

Guidance literature:

With potassium hydroxide; In ethanol; at 110 ℃; for 2h;

DOI:10.1016/j.tetasy.2006.05.001

upstream raw materials:

(-)-menthyl 2-exo-acetamidobicyclo<2.2.1>hept-5-ene-2-endo-carboxylate

N-Acetamidoacrylic acid

cyclopenta-1,3-diene

methyl 2-exo-acetamidobicyclo<2.2.1>hept-5-ene-2-endo-carboxylate

Downstream raw materials:

2-endo-Acetamido-2-exo-phenylethynylnorbornene

N-((1R,2S,4R)-2-Phenylethynyl-bicyclo[2.2.1]hept-5-en-2-yl)-acetamide

2-endo-Acetamido-2-exo-benzylthionorbornane

2-exo-Acetamido-2-endo-benzylthionorbornane

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