3-(3-AMINOPROPYL)SOLKETAL

Base Information

Chemical Name:3-(3-AMINOPROPYL)SOLKETAL
CAS No.:131606-42-3
Molecular Formula:C9H19NO3
Molecular Weight:189.255
Hs Code.:2932999099
Mol file:131606-42-3.mol

Synonyms:3-(3-AMINOPROPYL)SOLKETAL

Suppliers and Price of 3-(3-AMINOPROPYL)SOLKETAL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-(3-AMINOPROPYL)SOLKETAL

Chemical Property:

Boiling Point:279.9±25.0 °C(Predicted)
PKA:9.69±0.10(Predicted)
PSA：53.71000
Density:0.996±0.06 g/cm3(Predicted)
LogP:1.20360

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(3-AMINOPROPYL)SOLKETAL

There total 3 articles about 3-(3-AMINOPROPYL)SOLKETAL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 16418-26-1
3-(2,2-dimethyl-[1,3]dioxolan-4-yl-methoxy)-propionitrile.

: 131606-42-3
3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methoxy]propan-1-amine

Guidance literature:: 3-(2,2-dimethyl-[1,3]dioxolan-4-yl-methoxy)-propionitrile.; With sodium tetrahydroborate; cobalt(II) chloride; In methanol; at 0 ℃; for 1h;

With ammonia; In methanol; water;

Reference yield:

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 131606-42-3
3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methoxy]propan-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran

2: NaBH₄, CoCl₂ / methanol

With sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4039(00)61181-4

Reference yield:

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 131606-42-3
3-[(2,2-dimethyl-1,3-dioxolan-4-yl)methoxy]propan-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 2 h / 20 °C / Cooling with ice

1.2: 2 h / 20 °C / Cooling with ice

2.1: cobalt(II) chloride hexahydrate; sodium tetrahydroborate / methanol / 2 h / 20 °C / Cooling with ice

With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; sodium hydride; In tetrahydrofuran; methanol;